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<div id="f1h1j5f" class="blog-box"> <div class="5j15jfh" id="blog-img-slider" class=""> </div> <div id="jfjfj51" class="blog-content"> <h3>微波諧振腔微擾法在檢測分子篩積炭中的應用</h3> <div id="hhhhf1h" class="blog-meta"> <p><span id="ffj111j" class="meta-date">2017-09-05</span></p> </div> <p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">前言：</span></strong></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-indent: 32px;line-height: 1.75em;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">分子篩是一種重要的固體酸催化劑，在催化反應過(guò)程中有失活現象發(fā)生，其機理有以下幾種可能途徑：（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">1</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">）<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">毒物的吸附</strong>，堿性分子是酸性中心的毒物或抑止劑，這些分子可能以雜質(zhì)形式存在于原料中，也可能于反應過(guò)程中形成。原料中的金屬離子的沉積會(huì )直接覆蓋活性中心或堵塞催化劑微孔孔道的入口，引起嚴重的失活現象；（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">2</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">）<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">焦炭沉積</strong>，含碳物質(zhì)在反應過(guò)程中生成后，沉積并掩蓋了活性中心，或使催化劑孔道口變窄或堵塞，這將在本文中重點(diǎn)講述；（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">3</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">）催化劑本身的<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">化學(xué)變化</strong>，這類(lèi)機理包括（Ⅰ）<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">融結</strong>，<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">可導致固體催化劑的比表面積及孔容下降</strong>；（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 宋體">Ⅱ</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">）<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">催化劑組分的相轉化</strong>；（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 宋體">Ⅲ</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">）<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">催化劑中活性組分的升華或溶化</strong>；（Ⅳ）<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">催化劑各種組分間、或催化劑與反應物間發(fā)生化學(xué)反應，從而使活潑催化劑變成較穩定的、不甚活潑的物質(zhì)</strong>。</span></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;line-height: 27.2000007629395px;orphans: auto;text-align: justify;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;background-color: rgb(255, 255, 255)"><br/></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 16px;line-height: 24px;font-family: 楷體">“</span><strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 16px;line-height: 24px;font-family: 楷體">焦炭</span></strong><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 16px;line-height: 24px;font-family: 楷體">”</span><strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 16px;line-height: 24px;font-family: 楷體">沉積：</span></strong></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-indent: 32px;line-height: 1.75em;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">“焦炭”一般泛指在烴類(lèi)化合物催化轉化過(guò)程中形成、并沉積在催化劑表面上的含碳物質(zhì)。按</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">Wolf</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">及</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">Alfani</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">的觀(guān)點(diǎn)，<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">“焦炭”是單環(huán)和多環(huán)芳烴以脂肪族鏈或環(huán)烷鏈相聯(lián)結的各種烴類(lèi)的混合物的總稱(chēng)</strong>。其組成結構隨催化劑、反應條件、時(shí)間以及參與反應的反應物的組成而變化?！敖固俊钡纳蓹C理極為復雜，步驟眾多、反應系列繁雜，因所用催化劑</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">-</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">反應物系而大不相同。</span></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-indent: 32px;line-height: 1.75em;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">“焦炭”沉積往往伴有催化劑失活，雖然其間并非始終是平行的。強酸比弱酸，</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">Lewis</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">酸比</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">Bro</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">nsted</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">酸更有利于焦炭的生成，而過(guò)渡金屬的存在，也將加速焦炭的生成?！敖固俊背练e所導致的失活，大致有直接和間接兩類(lèi)機理：（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">1</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">）<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">直接機理，“焦炭”或其前身物在活性中心上形成后，就不可逆的吸附在該中心上，隨之阻礙了反應物參與反應</strong>；（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">2</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">）<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">間接機理，“焦炭”沉積在催化劑的孔道的孔口，使其窄化或完全堵塞，從而使反應物的擴散或進(jìn)入孔道受到阻礙</strong>。</span></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;line-height: 1.75em;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體"> 采用電磁光譜可以檢測到“焦炭”的生成，結合在線(xiàn)紅外光譜和拉曼光譜可以大致分析“焦炭”成分，但是光譜技術(shù)主要是基于局部分子篩樣品分析，結合</span><sup style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">13</sup>C<span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體">固體核磁可以更全面的分析分子篩孔道內“焦炭”成分，但是固體核磁花費較大而且效率不高，因此本文作者采用<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">微波諧振腔微擾法</strong>來(lái)分析分子篩中的“焦炭”成分，該法更加簡(jiǎn)便高效（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;color: rgb(34, 34, 34);background: white">Nature communications, 2017, 8(1): 514</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 宋體;color: rgb(34, 34, 34);background: white">，</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;color: rgb(34, 34, 34);background: white">DOI:</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;color: rgb(0, 112, 192);background: white">10.1038/s41467-017-00602-8</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體">）。</span></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;line-height: 27.2000007629395px;orphans: auto;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-align: center;background-color: rgb(255, 255, 255)"><img title="1528198664229931.jpg" alt="1.jpg" src="/Ueditor/php/upload/image/20180605/1528198664229931.jpg"/></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 16px;line-height: 24px;font-family: 楷體">論文解析：</span></strong></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;line-height: 27.2000007629395px;orphans: auto;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-align: center;background-color: rgb(255, 255, 255)"><img title="1528198669984565.jpg" alt="2.jpg" src="/Ueditor/php/upload/image/20180605/1528198669984565.jpg"/></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-align: center;line-height: 25.5px;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">圖</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">1. </span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">共振軌跡示意圖（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">a</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">），微波腔體示意圖（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">b</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">，</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">c</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">）。</span></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-indent: 32px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><br/></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-indent: 32px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px;line-height: 21px;font-family: 楷體">介電損失<span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">ε”=</span>Δ<em style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-style: italic"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">BW</span></em><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">/(2<em style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-style: italic">f</em><sub style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">0</sub><em style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-style: italic">AV<sub style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">s</sub></em>)，</span>其中Δ<em style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-style: italic"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">BW</span></em>如圖</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px;line-height: 21px">1a</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px;line-height: 21px;font-family: 楷體">所示計算，</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px;line-height: 21px">A</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px;line-height: 21px;font-family: 楷體">為常數，<em style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-style: italic"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">Vs</span></em>為腔體中樣品體積，<span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">f<sub style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">0</sub> </span>為原始諧振頻率。</span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;text-indent: 0em;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px;line-height: 21px;font-family: 楷體">注：<span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體;font-size: 14px;text-indent: 32px">微波諧振腔微擾法是一種測定物質(zhì)介電常數的方法，可以通過(guò)測定介電常數的變化來(lái)分析物質(zhì)的組成等。由于積炭與分子篩的介電常數存在差異，因此通過(guò)微波</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體;font-size: 14px;text-indent: 32px">諧振腔微擾法可以判斷分子篩的積<span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體;font-size: 14px;text-indent: 32px">炭</span>情況。</span></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;line-height: 27.2000007629395px;orphans: auto;text-align: justify;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;background-color: rgb(255, 255, 255)"><br/></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;line-height: 27.2000007629395px;orphans: auto;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-align: center;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體"><img title="1528198681783113.jpg" alt="3.jpg" src="/Ueditor/php/upload/image/20180605/1528198681783113.jpg"/>圖</span>2. <span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體">催化劑床層不同區域的催化劑透射表征圖和微波曲線(xiàn)。</span></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;line-height: 27.2000007629395px;orphans: auto;text-align: justify;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;background-color: rgb(255, 255, 255)"><br/></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-indent: 32px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">如圖</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">2</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">所示，</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">ZSM-5</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">催化劑呈現白色（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">2c</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">，</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">f</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">），經(jīng)過(guò)</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">5h</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">甲醇制烴反應后</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 宋體">，</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">催化劑床層上端積炭較多，催化劑顏色最深，通過(guò)高倍透射電鏡可以觀(guān)察到明顯的較大深色積炭區域（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">2a</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">，</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">d</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">），催化劑床層下端有少許積炭，催化劑顏色呈淺灰色，高倍透射電鏡顯示催化劑表面零散的分布深色“焦炭”（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">2b</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">，</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">e</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">，</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">g</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">）。<strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">微波曲線(xiàn)（</strong></span><strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px">2h</span></strong><strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;line-height: 21px;font-family: 楷體">）揭示積炭較多的上端催化劑諧振譜帶遷移更大而且更寬。</span></strong></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;text-indent: 0em;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important"></strong></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;line-height: 27.2000007629395px;orphans: auto;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-align: center;background-color: rgb(255, 255, 255)"><img title="1528198685492044.jpg" alt="4.jpg" src="/Ueditor/php/upload/image/20180605/1528198685492044.jpg"/></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;line-height: 27.2000007629395px;orphans: auto;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-align: center;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體">圖</span>3. <span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體">催化劑單位積炭重量的介電損失<span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">(ε”/wt%)</span>數據以及熱重和拉曼光譜。</span></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;text-indent: 0em;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 16px;font-family: 楷體"><br/></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;text-indent: 0em;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important"></strong></span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體"> 如圖</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">3</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體">所示，拉曼光譜分析揭示上端催化劑存在一個(gè)明顯的</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">1605cm<sup style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">-1</sup></span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體">特征峰，表明積炭主要以多環(huán)芳烴為主，下端催化劑在</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">1300</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體">和</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">1550cm<sup style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">-1</sup></span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體">之間吸收有所增強，可能是存在烯烴或脂肪烴沉積物所致。結合熱重和介電損失數據分析可知，上端催化劑單位積炭重量的介電損失<span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">(ε”/wt%)</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體">為</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">0.135</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體">，明顯大于下端催化劑（</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important">0.021</span><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體">）。</span></span></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;text-indent: 0em;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-family: 楷體"></span></span></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 16px;line-height: 24px;font-family: 楷體"><br/></span></strong></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;text-indent: 0px;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 16px;line-height: 24px;font-family: 楷體">總結：</span></strong></p><p style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;clear: both;min-height: 1em;color: rgb(51, 51, 51);font-family: 'Hiragino Sans GB', 'Microsoft YaHei', Arial, sans-serif;font-size: 17px;font-style: normal;font-variant: normal;font-weight: normal;letter-spacing: 0.544000029563904px;orphans: auto;text-align: justify;white-space: normal;widows: 1;word-spacing: 0px;-webkit-text-stroke-width: 0px;text-indent: 32px;line-height: 25.5px;background-color: rgb(255, 255, 255)"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important;font-size: 14px"><strong style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word !important"><span style=";padding: 0px;max-width: 100%;box-sizing: border-box !important;word-wrap: break-word 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